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Title:IDENTIFIKACIJA NEKATERIH TEHNIČNO POMEMBNIH POLIMEROV NA OSNOVI NJIHOVIH FIZIKALNO-KEMIJSKIH LASTNOSTI
Authors:ID Mežnar, Maja (Author)
ID Goršek, Andreja (Mentor) More about this mentor... New window
ID Pečar, Darja (Comentor)
Files:.pdf VS_Meznar_Maja_2016.pdf (1,00 MB)
MD5: A30473D7C80D6A9BAF64F1C51EFD7B2B
 
Language:Slovenian
Work type:Bachelor thesis/paper
Typology:2.11 - Undergraduate Thesis
Organization:FKKT - Faculty of Chemistry and Chemical Engineering
Abstract:Z raziskavami v sklopu diplomskega dela smo na osnovi njihovih fizikalno-kemijskih lastnosti identificirali različne polimere. Za njihovo preizkušanje smo uporabili različne laboratorijske metode: preizkus s segrevanjem in gorenjem, preizkus po Beilsteinu, preizkušanje topnosti v topilih in identifikacijo vzorca z infrardečo spektrometrijo. Z rezultati smo potrdili znano dejstvo, da so zgradbe enakih vrst polimerov med seboj podobne. Do manjših odstopanj v pričakovanih lastnostih je prihajalo le v primerih, ko so bili polimerom dodani različni aditivi, ki izboljšajo njihove lastnosti. Izvajali smo tudi kolonsko kromatografijo, ki je ena izmed metod ločevanja dveh ali več različnih polimerov. V našem primeru smo ločevali dva polimera. Najprej smo posneli njuna spektra. Nato smo oba polimera, raztopljena v ustreznih topilih, združili in posneli še spekter zmesi. Zmes smo spustili skozi kolono z omočenim silikagelom kot stacionarno fazo. Polimera sta se uspešno ločila, kar smo potrdili s posnetima spektroma obeh eluatov.
Keywords:polimeri, identifikacija, kolonska kromatografija, FTIR, silikagel
Place of publishing:Maribor
Publisher:[M. Mežnar]
Year of publishing:2016
PID:20.500.12556/DKUM-61112 New window
UDC:543.544.16:66.095.268(043.2)
COBISS.SI-ID:20369686 New window
NUK URN:URN:SI:UM:DK:KTV6G4UF
Publication date in DKUM:16.09.2016
Views:1940
Downloads:167
Metadata:XML DC-XML DC-RDF
Categories:KTFMB - FKKT
:
MEŽNAR, Maja, 2016, IDENTIFIKACIJA NEKATERIH TEHNIČNO POMEMBNIH POLIMEROV NA OSNOVI NJIHOVIH FIZIKALNO-KEMIJSKIH LASTNOSTI [online]. Bachelor’s thesis. Maribor : M. Mežnar. [Accessed 11 April 2025]. Retrieved from: https://dk.um.si/IzpisGradiva.php?lang=eng&id=61112
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Secondary language

Language:English
Title:IDENTIFICATION OF SOME IMPORTANT TECHNICAL POLYMERS BASED ON THEIR PHYSICO-CHEMICAL PROPERTIES
Abstract:The research was based on the physicochemical properties of various polymers. For their test, we used a variety of laboratory methods, such as examination by heating and burning, Beilstein test, testing the solubility in solvents and identification of the sample with infrared spectrometry. The results confirmed a known fact that structures of the same kinds of polymers are similar to each other. Minor variations in the expected properties were noticeable when various additives were added to the polymers to improve their properties. We have also carried out column chromatography, which is a method of separating two or more different polymers. In our case, we distinguished two polymers. First, we recorded their spectrum. Then, both polymers were dissolved in appropriate solvents and the spectrum of the mixture was combined and recorded. The mixture was passed through a column with the wetted silica gel as a stationary phase. Polymers were successfully separated, which was confirmed with recorded spectrum of both eluents.
Keywords:polymers, identification, column chromatography, FTIR, silica gel


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