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Title:Razvoj in uporaba analiznih metod določanja težkih kovin v okoljskih vzorcih z emisijsko spektrometrijo z induktivno skopljeno plazmo
Authors:Kavšek, Darja (Author)
Brodnjak-Vončina, Darinka (Mentor) More about this mentor... New window
Kolar, Mitja (Co-mentor)
Files:.pdf DOK_Kavsek_Darja_2015.pdf (3,60 MB)
MD5: 22A48EC579DEB48DA59AA0B83C985234
 
Language:Slovenian
Work type:Dissertation (m)
Typology:2.08 - Doctoral Dissertation
Organization:FKKT - Faculty of Chemistry and Chemical Engineering
Abstract:V doktorski disertaciji smo razvili, optimizirali in s pomočjo validacije potrdili analizne metode za točno in natančno določevanje izbranih težkih kovin v različnih matricah okoljskih vzorcev z optično emisijsko spektrometrijo z induktivno sklopljeno plazmo (ICP–OES). S pomočjo izmerjenih vsebnosti onesnaževal ter kemijskih in fizikalno–kemijskih parametrov smo izvedli kemometrijsko karakterizacijo različnih okoljskih vzorcev. Iskali smo korelacije med različnimi okoljskimi vzorci, ki so bili odvzeti na različnih vzorčnih mestih v različnih časovnih obdobjih.
Keywords:ICP–OES, premog, sedimenti, odpadne tekstilne vode, odpadne industrijske vode, težke kovine, validacija, kemometrijska klasifikacija, kemometrijska karakterizacija, analiza grupiranja, metoda glavnih osi, diskriminantna analiza
Year of publishing:2014
Publisher:[D. Kavšek]
Source:Maribor
UDC:543.42:549.25(043.3)
COBISS_ID:18358294 New window
NUK URN:URN:SI:UM:DK:KVDAAXNJ
Views:1826
Downloads:311
Metadata:XML RDF-CHPDL DC-XML DC-RDF
Categories:KTFMB - FKKT
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Secondary language

Language:English
Title:DEVELOPMENT AND USE OF ANALYTICAL METHODS FOR HEAVY METALS DETERMINATION IN ENVIRONMENTAL SAMPLES BY EMISSION SPECTROMETRY WITH INDUCTIVELY COUPLED PLASMA
Abstract:The present doctoral thesis was used to develop, optimise and, by means of validation, to confirm the analytical methods for accurate and precise determination of selected heavy metals in various matrices of environmental samples using inductively coupled plasma optical emission spectrometry (ICP–OES). Based on the measured content of pollutants, of both chemical and physical-chemical parameters, chemometric characterisation of different environment samples has been performed. We were interested in correlation between different environmental samples taken at different sampling points at different times.
Keywords:ICP–OES, coal, sediments, textile wastewaters, industrial wastewaters, heavy metals, validation, chemometric classification, chemometric characterisation, cluster analysis, principal component analysis, discriminant analysis


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