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Title:
OPTIMIZACIJA PROCESA KRISTALIZACIJE FARMACEVTSKE UČINKOVINE
Authors:
ID
Kiraly, Annamaria
(Author)
ID
Kravanja, Zdravko
(Mentor)
More about this mentor...
Files:
UNI_Kiraly_Annamaria_2010.pdf
(2,42 MB)
MD5: F6600279679CA53470392D4F93EF07D8
PID:
20.500.12556/dkum/846bef54-cc2f-49dd-8a6e-71925f4b0821
Language:
Slovenian
Work type:
Undergraduate thesis
Organization:
FKKT - Faculty of Chemistry and Chemical Engineering
Abstract:
V diplomski nalogi opisujemo eksperimentalno načrtovanje optimizacije kristalizacije farmacevtske učinkovine s Taguchijevo optimizacijsko metodo, ki jo že izvajajo v industrijskem merilu. Glede na kriterije optimiranja, ki so minimiziranje časa kristalizacije ob maksimiranju izkoristka in izboljšanju selektivnosti med produktom in nečistočami smo predpostavili, da na kristalizacijo vplivajo trije parametri in sicer hitrost ohlajanja, vrtilna frekvenca mešala in količina dodanih topil. Parametre kristalizacije smo proučevali na treh nivojih, njihov vpliv pa določali z analizo eksperimentalno dobljenih vrednosti optimizacijskih parametrov pri različnih pogojih eksperimenta s statistično metodo ANOVA.
Keywords:
optimiranje
,
Taguchijeva metoda
,
kristalizacija
,
industrijski proces
Place of publishing:
Maribor
Publisher:
[A. Kiraly]
Year of publishing:
2010
PID:
20.500.12556/DKUM-15880
UDC:
66.065.5:548(043.2)
COBISS.SI-ID:
14394646
NUK URN:
URN:SI:UM:DK:5LY9YUHW
Publication date in DKUM:
28.09.2010
Views:
2767
Downloads:
315
Metadata:
Categories:
KTFMB - FKKT
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:
KIRALY, Annamaria, 2010,
OPTIMIZACIJA PROCESA KRISTALIZACIJE FARMACEVTSKE UČINKOVINE
[online]. Bachelor’s thesis. Maribor : A. Kiraly. [Accessed 2 April 2025]. Retrieved from: https://dk.um.si/IzpisGradiva.php?lang=eng&id=15880
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Secondary language
Language:
English
Title:
OPTIMIZATION OF A PROCESS OF CRYSTALIZATION OF A PHARMACEUTICAL SUBSTANCE
Abstract:
An optimization of crystallization of a pharmaceutical substance, which is already produced in the industry, is described in this work. The purpose of the study, was to determine the influence of different process parameters on product quality, their optimal values and the end of crystallization, for what we used Taguchi optimization method. We assumed that the crystallizaton is most affected by three parameters, which are the cooling rate, stirrer speed and the amount of added solvent. Crystallization parameters were studied at three levels and analized with the statistical method ANOVA.
Keywords:
optimization
,
Taguchi method
,
crystallization
,
industrial process
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