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Title:Sinteza koordinacijskih spojin železa s piridinkarboksamidi (pikolinamid, nikotinamid, izonikotinamid)
Authors:ID Babič, Nejc (Author)
ID Kristl, Matjaž (Mentor) More about this mentor... New window
ID Dojer, Brina (Co-mentor)
Files:.pdf MAG_Babic_Nejc_2018.pdf (8,04 MB)
MD5: 0972ADACB914B91BC859AB8C11611649
PID: 20.500.12556/dkum/e5db7520-f24f-4590-8a4e-af54e4299b78
Work type:Master's thesis/paper
Typology:2.09 - Master's Thesis
Organization:FNM - Faculty of Natural Sciences and Mathematics
Abstract:Namen magistrskega dela je bila sinteza in karakterizacija novih koordinacijskih spojin železa z izbranimi piridinkarboksamidi (pikolinamid, nikotinamid in izonikotinamid). Opravljenih je bilo 20 sintez, pri katerih smo spreminjali sintezne pogoje in izbrane reagente. Najpogosteje uporabljeno topilo je bilo metanol. Sintezne produkte smo karakterizirali z rentgensko praškovno difrakcijo, infrardečo spektroskopijo in strukturno analizo na monokristalu. Uspelo nam je sintetizirati novo koordinacijsko spojino s kemijsko formulo (isnH)2[Fe(isn)2(SO4)2(H2O)2]·H2O, katere struktura do sedaj še ni bila opisana. Spojina je bila produkt dveh sintez (NB19 in NB20), pri katerih smo kot reagenta uporabili izonikotinamid in železov(II) sulfat heptahidrat. Sintezi smo izvedli z mešanjem pod refluksom.
Keywords:koordinacijska spojina, ligand, železo, piridinkarboksamidi, izonikotinamid, rentgenska praškovna difrakcija, Fourierjeva transformacijska infrardeča spektroskopija, monokristalna analiza.
Place of publishing:Maribor
Publisher:[N. Babič]
Year of publishing:2018
PID:20.500.12556/DKUM-72797 New window
COBISS.SI-ID:24231688 New window
Publication date in DKUM:13.12.2018
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License:CC BY-NC-ND 4.0, Creative Commons Attribution-NonCommercial-NoDerivatives 4.0 International
Description:The most restrictive Creative Commons license. This only allows people to download and share the work for no commercial gain and for no other purposes.
Licensing start date:19.11.2018

Secondary language

Title:Synthesis of iron coordination compounds with pyridine carboxamides
Abstract:The purpose of this Master thesis was the synthesis and characterization of the new iron coordination compounds with pyridinecarboxamides (picolineamide, nicotinamide and isonicotinamide). We performed 20 synthesis, in which we changed conditions and the selected reagents. The most commonly used solvent was methanol. The synthesis products were characterized by X-ray powder diffraction, infrared spectroscopy and single-crystal X-ray diffraction. We succeeded to synthesize new coordination compound with chemical formula (isnH)2[Fe(isn)2(SO4)2(H2O)2]·H2O. The compound´s structure has not yet been known. It was the synthesis product of two syntheses (NB19 in NB20), where the isonicotinamide and iron (II) sulphate heptahydrate were used as the reagent. The compound was synthesized by stirring under reflux.
Keywords:coordination compound, ligand, iron, pyridinecarboxamides, isonicotinamid, X-ray powder diffraction, Fourier transform infrared spectroscopy, single-crystal X-ray diffraction.


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