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Title:Sinteza in karakterizacija bakrovih koordinacijskih spojin z izbranimi tio-liganidi
Authors:Rozman, Ana (Author)
Kristl, Matjaž (Mentor) More about this mentor... New window
Dojer, Brina (Co-mentor)
Files:.pdf MAG_Rozman_Ana_2018.pdf (4,34 MB)
 
Language:Slovenian
Work type:Master's thesis/paper (mb22)
Typology:2.09 - Master's Thesis
Organization:FNM - Faculty of Natural Sciences and Mathematics
Abstract:Namen magistrskega dela je bila sinteza in karakterizacija novih koordinacijskih spojin z bakrom. Pri tem so bili kot reagenti uporabljeni bakrov(II) acetat monohidrat in različni tio-ligandi. Sinteze so bile izvedene z mešanjem pri sobni temperaturi, z mešanjem pod refluksom ali solvotermalno, pri povišani temperaturi in tlaku. Pri pripravi raztopin reagentov sta bili najpogosteje uporabljeni topili metanol in N,N-dimetilformamid (DMF). Izvedenih je bilo 36 sintez. Sintezne produkte smo karakterizirali z infrardečo spektroskopijo, rentgensko praškovno difrakcijo in rentgensko strukturno analizo na monokristalu. Uspelo nam je sintetizirati spojino 6-aminopiridin-3-karbonitril, s kemijsko formulo C6H5N3, katere struktura do sedaj še ni bila znana. Spojino smo sintetizirali pri dveh izvedenih sintezah, prvič solvotermalno, kjer je bil kot topilo uporabljen metanol in drugič z mešanjem pod refluksom, kjer sta bili kot topili uporabljeni metanol in DMF.
Keywords:koordinacijska spojina, baker, bakrov(II) acetat monohidrat, tio-ligandi, 6-aminopiridin-3-karbonitril, infrardeča spektroskopija s Fourierjevo transformacijo (FTIR), rentgenska praškovna difrakcija (XRD), monokristalna analiza
Year of publishing:2018
Publisher:[A. Rozman]
Source:Maribor
UDC:546.562:543.427(043.2)
COBISS_ID:24010760 Link is opened in a new window
NUK URN:URN:SI:UM:DK:WNW2DNUK
License:CC BY-NC-ND 4.0
This work is available under this license: Creative Commons Attribution Non-Commercial No Derivatives 4.0 International
Views:275
Downloads:31
Metadata:XML RDF-CHPDL DC-XML DC-RDF
Categories:FNM
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Secondary language

Language:English
Title:Synthesis and characterization of coordination compounds with copper using thio-liganids
Abstract:The purpose of this work was the synthesis and characterization of the new copper coordination compounds. Copper(II) acetate monohydrate and different thio-ligands were used as the chemical reagents. Synthesis reactions were performed by stirring at room temperature, by stirring under reflux or solvothermal at high temperature and pressure. We commonly used methanol and N,N-dimethylformamide as solvents. We performed 36 synthesis reactions. The synthesis products were characterized by infrared spectroscopy, X-ray powder diffraction and single-crystal X-ray diffraction. We succeeded in the synthesis of 6-aminopyridine-3-carbonitrile with chemical formula C6H5N3. The compound’s structure has not yet been known. The compound was synthesized twice; first by solvothermal synthesis with methanol as solvent and second by stirring under reflux with methanol and DMF as solvents.
Keywords:coordination compound, copper, copper(II) acetate monohydrate, thio-ligands, 6-aminopyridine-3-carbonitrile, Fourier-transform infrared spectroscopy (FTIR), X-ray powder diffraction, single-crystal X-ray diffraction


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