Naslov: | Synthesis of nickel and cobalt sulfide nanoparticles using a low cost sonochemical method |
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Avtorji: | ID Kristl, Matjaž (Avtor) ID Dojer, Brina (Avtor) ID Gyergyek, Sašo (Avtor) ID Kristl, Janja (Avtor) |
Datoteke: | Heliyon_2017_Kristl_et_al._Synthesis_of_nickel_and_cobalt_sulfide_nanoparticles_using_a_low_cost_sonochemical_method.pdf (2,41 MB) MD5: ABE6E8A6F483F9E4D6DE79275B10722B PID: 20.500.12556/dkum/b58c4226-841d-4f4c-8eec-a6be3fadbc9d
http://www.heliyon.com/article/e00273
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Jezik: | Angleški jezik |
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Vrsta gradiva: | Znanstveno delo |
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Tipologija: | 1.01 - Izvirni znanstveni članek |
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Organizacija: | FKKT - Fakulteta za kemijo in kemijsko tehnologijo
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Opis: | Nickel and cobalt sulfides are promising materials in different cutting-edge research areas like solar cells, supercapacitors, catalysts, and electrode materials. Nickel and cobalt sulfides with various stoichiometries have been synthesized sonochemically from $Ni(CH_3COO)_2$ ∙ $4H_2O$, $Co(CH_3COO)_2$ ∙ $2H_2O$ and different sulfur precursors using a direct immersion ultrasonic probe. The products were characterized by X-ray powder diffraction, transmission electron microscopy (TEM) including EDX analysis, IR and UV–Vis spectroscopy and elemental analysis. Following products have been obtained: $NiS$, $Ni_3S_4$, $CoS_{1.097}$ and $Co_9S_8$, with average crystallite sizes in the range 7−30 nm. Effects of different reaction conditions on the size, morphology and optical band-gap energy were evaluated. Optical band-gap energies in the range 3.3 eV−3.8 eV were observed for the obtained nanoparticles. |
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Ključne besede: | material science, inorganic chemistry, nanotechnology |
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Status publikacije: | Objavljeno |
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Verzija publikacije: | Objavljena publikacija |
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Leto izida: | 2017 |
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Št. strani: | str. 1-19 |
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Številčenje: | Letn. 3, št. 3 |
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PID: | 20.500.12556/DKUM-66884 |
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ISSN: | 2405-8440 |
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UDK: | 54 |
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COBISS.SI-ID: | 20516118 |
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DOI: | 10.1016/j.heliyon.2017.e00273 |
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ISSN pri članku: | 2405-8440 |
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NUK URN: | URN:SI:UM:DK:5F8D67AQ |
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Datum objave v DKUM: | 14.07.2017 |
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Število ogledov: | 1644 |
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Število prenosov: | 404 |
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Metapodatki: | |
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Področja: | Ostalo
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Vaša ocena: | Ocenjevanje je dovoljeno samo prijavljenim uporabnikom. |
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