| | SLO | ENG | Cookies and privacy

Bigger font | Smaller font

Show document

Title:MEHANOKEMIJSKE SINTEZE SULFIDOV PREHODNIH KOVIN 4. PERIODE (MxSy; M = Zn, Ni, Co)
Authors:ID Lečnik, Katja (Author)
ID Kristl, Matjaž (Mentor) More about this mentor... New window
ID Ban, Irena (Co-mentor)
Files:.pdf VS_Lecnik_Katja_2016.pdf (2,22 MB)
MD5: 0A1FDC81CC5F83A4486198CF07ADC536
 
Language:Slovenian
Work type:Bachelor thesis/paper (mb11)
Typology:2.11 - Undergraduate Thesis
Organization:FKKT - Faculty of Chemistry and Chemical Engineering
Abstract:Diplomsko delo prikazuje študijo sintetiziranja sulfidov prehodnih kovin 4. periode (MxSy; M = Zn, Ni, Co) s pomočjo mehanokemijske metode. Pri tem smo uporabljali visokoenergijski kroglični mlin SPEX 8000M. Vzorce, dobljene z mletjem, smo analizirali s pomočjo rentgenske praškovne difrakcije (XRD), za segrevanje nekaterih produktov pa smo uporabili napravo za termogravimetrično analizo (TGA). Namen te študije je bil spoznavanje mehanokemijskih metod, rentgenske praškovne difrakcije in aparata za termogravimetrično analizo. To diplomsko delo opisuje rezultate vseh izvedenih sintez in metode s katerimi smo prišli do teh rezultatov. Ugotovili smo, da je uporaba mehanokemjskih metod za sintezo sulfidov prehodnih kovin 4. periode lahko učinkovita.
Keywords:mehanokemijska sinteza, rentgenska praškovna difrakcija, mlin SPEX 8000M, cinkov sulfid, nikljev sulfid, kobaltov sulfid, mletje
Year of publishing:2016
Publisher:[K. Lečnik]
Source:Maribor
PID:20.500.12556/DKUM-62339 New window
UDC:544.463(043.2)
COBISS.SI-ID:20313110 New window
NUK URN:URN:SI:UM:DK:TOSJCKPU
Publication date in DKUM:17.10.2016
Views:1097
Downloads:109
Metadata:XML RDF-CHPDL DC-XML DC-RDF
Categories:KTFMB - FKKT
:
  
Average score:(0 votes)
Your score:Voting is allowed only for logged in users.
Share:AddThis
AddThis uses cookies that require your consent. Edit consent...

Hover the mouse pointer over a document title to show the abstract or click on the title to get all document metadata.

Secondary language

Language:English
Title:MECHANOCHEMICAL SYNTHESIS OF SULFIDES WITH TRANSITION METALS FROM 4. PERIOD (MxSy; M = Zn, Ni, Co)
Abstract:This diploma thesis studies the synthesis of sulfides with transition metals from 4. period (MxSy; M = Zn, Ni, Co) by using the mechanochemical method. We used a high energy ball mill SPEX 8000M. Samples, obtained by milling, were analyzed using X-ray powder diffraction (XRD), for heating of some products we used a device for thermogravimetric analysis (TGA). The purpose of this study was to get familiar with mechanochemical methods, X-ray powder diffraction and the machine for thermogravimetric analysis. This thesis describes the results of performed syntheses and methods that got us to those results. We found that mechanochemical synthesis of sulfides with transition metals from 4. period can be effective.
Keywords:mechanochemical synthesis, XRD, mill SPEX 8000M, zinc sulfide, nickel sulfide, cobalt sulfide, ball-milling


Comments

Leave comment

You must log in to leave a comment.

Comments (0)
0 - 0 / 0
 
There are no comments!

Back
Logos of partners University of Maribor University of Ljubljana University of Primorska University of Nova Gorica