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Title:DOLOČANJE ADSORBLJIVIH ORGANSKIH HALOGENOV V ODPADNIH VODAH
Authors:ID Marot, Nina (Author)
ID Brodnjak-Vončina, Darinka (Mentor) More about this mentor... New window
ID Kolar, Mitja (Comentor)
ID Zagajšek, Aleš (Comentor)
Files:.pdf VS_Marot_Nina_2013.pdf (1,95 MB)
MD5: BB0841D6822F80DD9DC5EC3D396C4D21
PID: 20.500.12556/dkum/3f16e93b-f0e5-4e97-9c97-f8a526929266
 
Language:Slovenian
Work type:Undergraduate thesis
Typology:2.11 - Undergraduate Thesis
Organization:FKKT - Faculty of Chemistry and Chemical Engineering
Abstract:Namen diplomskega dela je validacija analizne metode za določevanje adsorbljivih organskih halogenov (AOX) v odpadnih vodah. Proces validacije zajema določitev validacijskih parametrov z izdelavo validacijskega načrta. Sledi eksperimentalna izvedba validacije ter statistično pridobljenih rezultatov. Določili smo potrditev identitete in selektivnost oziroma specifičnost, delovno in linearno območje, mejo zaznavnosti, mejo določljivosti, LOQ v matrici, zgornjo mejo določanja v matrici, vpliv redčenja vzorcev, točnost, natančnost in vpliv matrice. Analizirani so bili tudi realni vzorci bazenskih, bolnišničnih odpadnih vod ter odpadne vode iz iztoka iz čistilnih naprav. Na podlagi vseh pridobljenih rezultatov ter na predpisane parametre smo potrdili, da izbrana analizna metoda izpolnjuje predpisane pogoje ter zagotavlja pravilnost in zanesljivost rezultatov.
Keywords:AOX, validacija analizne metode, odpadne vode, adsorpcija
Place of publishing:Maribor
Publisher:[N. Marot]
Year of publishing:2013
PID:20.500.12556/DKUM-39882 New window
UDC:543.2/.9:628.166(043.2)
COBISS.SI-ID:17461014 New window
NUK URN:URN:SI:UM:DK:O48PNNAG
Publication date in DKUM:29.03.2013
Views:2786
Downloads:293
Metadata:XML DC-XML DC-RDF
Categories:KTFMB - FKKT
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Secondary language

Language:English
Title:DETERMINATION OF ADSORBABLE ORGANICALLY BOUND HALOGENS IN WASTE WATERS
Abstract:The purpose of the this thesis was the validation of the analytical method for the determination of adsorbable organically bound halogens (AOX) in waste waters. Validation process comprises determination of validation parameters and the validation plan. After the validation plan an experimental part of the validation with the statistically of results was performed. We have also confirmed the identity and determined selectivity and specificity, working and linear range, limit of detection LOD, limit of quantitation, LOQ in the matrix, the upper limit of the matrix, the impact of dilution samples, accuracy, precision and matrix effect. We also analysed real samples, a pool water, a hospital waste water and a waste water from effluent treatment plants. On the basis of results obtained according to the prescribed parameters, it was confirmed that this analytical method complies with the conditions prescribed and ensures the accuracy and reliability of the results.
Keywords:AOX, validation of analytical methods, waste water, adsorption


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