| Title: | Hydroxylammonium fluorogermanates |
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| Authors: | ID Ban, Irena (Author)
ID Kristl, Matjaž (Author)
ID Drofenik, Mihael (Author)
ID Popović, Arkadije (Author) |
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| Files: |  http://dx.doi.org/10.1016/j.tca.2004.02.016
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| Language: | English |
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| Work type: | Unknown |
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| Typology: | 1.01 - Original Scientific Article |
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| Organization: | FKKT - Faculty of Chemistry and Chemical Engineering
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| Abstract: | A new hydroxylammonium compound (NH3OH)2GeF6, has been synthesized by the addition of solid NH3OHF to a solution of GeO2 dissolved in 20% HF. The compound was characterized by chemical analysis and X-ray powder diffraction, the thermal decomposition was studied by thermal analysis and mass spectrometry. (NH3OH)2GeF6 crystallizes monoclinic. Two endothermic and two exothermic peaks have been observed on the DSC curve, the decomposition product at 500 °C is GeO2. |
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| Keywords: | inorganic chemistry, synthesis, characterisation, hydroxylammonium fluorogermanates, x-ray powder diffraction, mass spectroscopy, thermal analysis |
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| Year of publishing: | 2004 |
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| PID: | 20.500.12556/DKUM-27511  |
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| UDC: | 541.49.057:548.73 |
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| ISSN on article: | 0040-6031 |
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| COBISS.SI-ID: | 8703766 |
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| NUK URN: | URN:SI:UM:DK:JI7RDUZP |
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| Publication date in DKUM: | 01.06.2012 |
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| Views: | 3353 |
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| Downloads: | 115 |
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| Metadata: |    |
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| Categories: | Misc.
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