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Title:Hydroxylammonium fluorogermanates
Authors:ID Ban, Irena (Author)
ID Kristl, Matjaž (Author)
ID Drofenik, Mihael (Author)
ID Popović, Arkadije (Author)
Files:URL http://dx.doi.org/10.1016/j.tca.2004.02.016
 
Language:English
Work type:Unknown ()
Typology:1.01 - Original Scientific Article
Organization:FKKT - Faculty of Chemistry and Chemical Engineering
Abstract:A new hydroxylammonium compound (NH3OH)2GeF6, has been synthesized by the addition of solid NH3OHF to a solution of GeO2 dissolved in 20% HF. The compound was characterized by chemical analysis and X-ray powder diffraction, the thermal decomposition was studied by thermal analysis and mass spectrometry. (NH3OH)2GeF6 crystallizes monoclinic. Two endothermic and two exothermic peaks have been observed on the DSC curve, the decomposition product at 500 °C is GeO2.
Keywords:inorganic chemistry, synthesis, characterisation, hydroxylammonium fluorogermanates, x-ray powder diffraction, mass spectroscopy, thermal analysis
Year of publishing:2004
PID:20.500.12556/DKUM-27511 New window
UDC:541.49.057:548.73
ISSN on article:0040-6031
COBISS.SI-ID:8703766 New window
NUK URN:URN:SI:UM:DK:JI7RDUZP
Publication date in DKUM:01.06.2012
Views:2145
Downloads:93
Metadata:XML RDF-CHPDL DC-XML DC-RDF
Categories:Misc.
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Record is a part of a journal

Title:Thermochimica acta
Shortened title:Thermochim. acta
Publisher:Elsevier
ISSN:0040-6031
COBISS.SI-ID:832516 New window

Secondary language

Language:English
Keywords:anorganska kemija, sinteze, karakterizacija, hidroksilamonijevi fluorogermanati, rentgenska praškovna analiza, masna spektroskopija, termična analiza


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