| Naslov: | Influence of temperature and pressure during PGSS[sup]TM micronization and storage time on degree of crystallinity and crystal forms of monostearate and tristearate |
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| Avtorji: | ID Mandžuka, Zoran (Avtor)
ID Knez, Željko (Avtor) |
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| Datoteke: |  http://dx.doi.org/10.1016/j.supflu.2007.11.006
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| Jezik: | Angleški jezik |
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| Vrsta gradiva: | Neznano |
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| Tipologija: | 1.01 - Izvirni znanstveni članek |
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| Organizacija: | FKKT - Fakulteta za kemijo in kemijsko tehnologijo
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| Opis: | For controlling the degree of crystallinity and crystal form during particle formation using supercritical fluids, knowledge of pressure influence on solid-liquid-gas (S-L-G) equilibrium and solubility data of the system is crucial. S-L-G equilibrium data were determined in pressure range from 50 to 600 bar for systems monostearate/CO2 and tristearate/CO2 using a high-pressure view cell. Results showed a temperature minimum for both systems.The solubilities of CO2 in liquid glycerides were high: maximum solubilities, which were determined at temperatures 70 and 90 °C and pressure range from 50 to 450 bar, were from 50 to 90 mol%. Physical characteristics of micronized monostearate and tristearate samples were studied in detail after micronization and after 3 months of storage at 20 °C. |
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| Ključne besede: | chemical processing, high pressure technology, supercritical fluids, micronization, fine particles, Particles from Gas Saturated Solution, degree of crystallinity |
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| Leto izida: | 2008 |
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| PID: | 20.500.12556/DKUM-26170  |
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| UDK: | 66-987 |
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| COBISS.SI-ID: | 12228886 |
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| ISSN pri članku: | 0896-8446 |
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| NUK URN: | URN:SI:UM:DK:L2S3PSVE |
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| Datum objave v DKUM: | 31.05.2012 |
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| Število ogledov: | 2958 |
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| Število prenosov: | 58 |
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| Metapodatki: |    |
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| Področja: | Ostalo
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