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Synthesis and characterisation of hydroxylammonium fluorochromate
Matjaž Kristl, Mihael Drofenik, Ljubo Golič, Amalija Golobič, 2003, izvirni znanstveni članek

Opis: Reactions in the system $Cr – NH_3OHF – HF – H_2O$ were investigated. Green crystals of a new compound with the formula $(NH_3OH)_3CrF_6$ have been isolated from the water solution and characterized by chemical analysis. The compound crystallizes as triclinic, P-1, with cell parameters: a = 6.5461(2) Å, b = 6.9347(2) Å, c = 9.4072(3) Å, α = 86.772(1)°, β = 83.804(1)°, γ = 70.283(1)°. The effective magnetic moment, $µ_{eff}$ = 3.82 BM, was calculated from magnetic susceptibility measurements in the temperature range 80-290 K. The thermal decomposition of the compound was studied by TG and DSC analysis. $(NH_3OH)_3CrF_6$ decomposes above 125 °C in three steps and the residue has been identified by X-ray powder diffraction as $α – Cr_2O_3$.
Ključne besede: inorganic chemistry, structural chemistry, crystalline structure, coordination compounds, synthesis, inorganic reactions, thermal decomposition, characterization of compounds, TG, DSC, X-ray diffraction, chromium complexes, hydroxylammonium fluoro chromates, crystals
Objavljeno: 25.08.2017; Ogledov: 919; Prenosov: 80
.pdf Celotno besedilo (206,45 KB)
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Experimental determination of fatigue parameters of high chromium steel under different loading and temperature conditions
Matej Drobne, Nenad Gubeljak, Srečko Glodež, 2014, izvirni znanstveni članek

Opis: Fatigue investigation of high chromium steel (HCS) at different loading ratios (R = 0, R = -1) and different temperatures (20 °C, 600 °C) is presented in this paper. Before fatigue testing, monotonic mechanical properties (ultimate compressive and ultimate tensile strength) are determined at different temperatures, using standardized testing procedures according to DIN 50125 standard. Moreover Charpy impact tests at different temperatures were done with specimens that comply with the standard ISO 14556. Fatigue testing is performed on a servo - hydraulic testing machine with consideration of different loading conditions as described above. On the basis of the experimental results the S - N curves are constructed from which typical fatigue parameters (the fatigue strength coefficient 0'f and the fatigue strength exponent b) are determined. After fatigue testing a comprehensive investigation of fracture surfaces is performed using the Scanning Electron Microscope (SEM). Experimental results presented in this paper will serve as a basis for further investigations related to fatigue behaviour of real working rolls in hot strip mills made of HCS.
Ključne besede: experiments, high chromium steel, high cycle fatigue, fracture mechanics
Objavljeno: 12.07.2017; Ogledov: 517; Prenosov: 99
.pdf Celotno besedilo (2,88 MB)
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Fatigue crack growth and fracture mechanics analysis of a working roll surface layer material
Matej Drobne, Tomaž Vuherer, Ivan Samardžić, Srečko Glodež, 2014, izvirni znanstveni članek

Opis: Fatigue crack growth and fracture mechanics analysis of a working roll surface layer material is presented in this paper. The research is done on a hot strip mill working roll where High Chromium Steel is used for roll’s shell material. To obtain corresponding parameters, a rectangular single edge notched bend specimens – SENB, according to standard BS 7448, were used. The fatigue crack growth analysis was done on a resonant testing machine with use of special crack gauges, while for fracture mechanics parameters the electro–mechanical testing machine was used.
Ključne besede: fracture mechanics, fatigue crack growth, metal forming, rolling process, high chromium steel
Objavljeno: 03.07.2017; Ogledov: 497; Prenosov: 81
.pdf Celotno besedilo (1,11 MB)
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