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Reactive sintering of $MnZn$ ferrites
Tomaž Kosmač, Mihael Drofenik, 2001, izvirni znanstveni članek

Opis: Reaction-formed $MnZn$ ferrite was prepared and the decrease in shrinkage after sintering due to the volume expansion accompanying iron oxidation was studied. Green compacts consisting of the milled raw oxides $Fe_2O_3$, $Mn_3O_4$, $ZnO$ and metallic iron powder were sintered at 1350 °C in air. During the first hold at 800 °C, $Fe$ was oxidized to $\alpha-Fe_2O_3$ and $Zn$ ferrite was formed. Above 1300 °C the reaction bonding was completed and $MnZn$ ferrite, exhibiting a relatively low shrinkage, was formed. The chemical reactions involved during reaction bonding were associated with a volume expansion and porosity formation, compensating for the shrinkage on sintering. Intensive milling decreases the porosity after sintering but induces the oxidation of iron, and partially removes the shrinkage compensation caused by the presence of metallic iron.
Ključne besede: reaction-forming, $MnZn$ ferrite, inorganic technology, ferrite ceramics, reaction bonded ceramics, sintering, iron oxides, iron
Objavljeno: 25.08.2017; Ogledov: 505; Prenosov: 68
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The characterisation of nanosized nickel-zinc ferrites synthesized within reverse micelles of CTAB/1-hexanol/water microemulsion
Vuk Uskoković, Mihael Drofenik, Irena Ban, 2004, izvirni znanstveni članek

Opis: Stoichiometric nanocrystalline nickel-zinc ferrites were synthesized by a reverse micelle method following a multi-microemulsion approach. Different pH values were chosen for the alkali precipitating reaction during the synthesis of different powders. Synthesized, as-dried and subsequently calcined powders were characterized in terms of their magnetic properties. XRD analyses and specific-surface area measurements were used to determine the average particlesizes of the synthesized samples. DCS and TGA measurements were performed to reveal the phase transitions within the samples at elevated temperatures, whereas TEM was used to view and record the microstructure of the nanosized ferrite samples. A possible mechanism of the formation of the synthesized NiZn-ferrite was also discussed.
Ključne besede: magnetic materials, magnetic nanoparticles, microemulsion synthesis, nickel, iron, fine powders, Ni-Zn ferrites, reverse micelle method
Objavljeno: 01.06.2012; Ogledov: 1391; Prenosov: 22
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Crystal-structure and Mössbauer studies of Li[sub]1.746]Nd[sub]4.494FeO9[sub]9.493
Mihael Drofenik, Irena Ban, Darko Makovec, Darko Hanžel, Amalija Golobič, Ljubo Golič, 2007, izvirni znanstveni članek

Opis: The ▫$Li_1.746Nd_4.494FeO_9.493$▫ (LNF) ternary phase, located in the ▫$Li_2O$▫-rich part of the ▫$Li_2O-Nd_2O_3-Fe_2O_3$▫ system, crystallizes with a cubic unit cell of dimension and the space group Im3m. Refinement on F resulted in R=1.9%. The structure is comprised of a network of corners, edges and faces sharing the coordination polyhedra of neodymium. In between this skeleton the regular octahedra of oxygen-coordinated iron and trigonal prisms of lithium are located. The Mössbauer spectra revealed the presence of ▫$Fe^3+$▫, ▫$Fe^4+$▫ and ▫$Fe^5+$▫ ions distributed on two symmetry-independent lattice positions.
Ključne besede: crystal structure, ternary compounds, single-crystal X-ray diffraction, Mössbauer spectroscopy, iron oxidation state, kristalna struktura, ternarne spojine, rentgenska difrakcija, Mössbauerjeva spektroskopija, rentgenska strukturna analiza
Objavljeno: 01.06.2012; Ogledov: 1585; Prenosov: 37
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Additive fabrication in metallurgy - case study of grey cast iron valve production
Bogdan Valentan, Igor Drstvenšek, Tomaž Brajlih, Peter Sever, Simon Brezovnik, Jože Balič, 2010, strokovni članek

Opis: Additive Fabrication technologies are well known from the last two decades. In that time Additive Fabrication technologies have evolved from strictly prototype part production into an option that can also be used to produce end-user parts. With development of Additive Fabrication machines capable of producing metal parts, a complete substitution of conventional metal casting technologies is possible. However, direct Additive Fabrication of metal parts is still not time/cost effective when producing large volume parts, and nowadays there is still lack of materials that can be used on those machines. This paper presents a method how a conventional sand casting process can be assisted by Additive Fabrication technologies. A sand mould pattern is produced by Selective Laser Sintering. Additive Fabrication is also used in direct manufacturing of cores.
Ključne besede: gray cast iron, layered technologies, rapid prototyping, rapid manufacturing, sand casting
Objavljeno: 31.05.2012; Ogledov: 1580; Prenosov: 15
URL Povezava na celotno besedilo

Dynamic two-axis model of a linear synchronous reluctance motor based on current and position-dependent characteristics of flux linkages
Gorazd Štumberger, Bojan Štumberger, Drago Dolinar, 2006, izvirni znanstveni članek

Opis: This paper analyses the impact of armature slotting and magnetically nonlinearand anisotropic iron core on the trajectories of a kinematically controlled linear synchronous reluctance motor (LSRM). A new magnetically nonlinear dynamic two-axis LSRM model is introduced in order to perform the analysis. The magnetic nonlinearities and slotting effects are accounted for by the current and position-dependent characteristics of flux linkages.
Ključne besede: devices motors, reluctance synchronous motor, iron core model
Objavljeno: 31.05.2012; Ogledov: 1795; Prenosov: 82
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The synthesis of iron-nickel alloy nanoparticles using a reverse micelle technique
Irena Ban, Mihael Drofenik, Darko Makovec, 2006, izvirni znanstveni članek

Opis: Nanosized Fe0.2Ni0.8 particles were prepared by reducing their salts with sodium borohydride (NaBH4) in cationic water-in-oil (w/o) microemulsions of water/cetyl-trimethyl-amonium bromide (CTAB) and n-butanol/isooctane at 25 °C.According to the TEM and X-ray diffraction analyses, the synthesized particles were around 4-12 nm in size. Due to their nanodimensions, the particles had a primitive cubic (pc) structure rather than the body-centered cubic (BCC) structure of the bulk material. An examination of the synthesis from the reverse micelle reveals that the morphology of the iron-nickel alloy nanoparticles depends mainly on the microemulsion`s composition. The magnetization of the nanoparticles was much lower than that of the bulk material, reflecting the influence of the nanodimensions on the particlesć magnetizations.
Ključne besede: magnetic materials, nickel/iron alloys, nanoparticles, synthesis, microemulsions, magnetic properties, reverse micelles
Objavljeno: 31.05.2012; Ogledov: 1495; Prenosov: 84
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