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Vial wall effect on freeze-drying speed
Matjaž Ramšak, Matjaž Hriberšek, 2024, izvirni znanstveni članek

Opis: The vial wall thermal conductivity and thickness effect on freeze-drying speed is simulated. A 2D axisymmetric numerical simulation of Mannitol freeze-drying is employed using the boundary element method. The originality of the presented approach lies in the simulation of heat transfer in the vial walls as an additional computational domain in contrast to the typical methodology without a vial wall. The numerical model was validated using our measurements and the measurements from the literature. Increasing the glass vial thickness from 1 mm to 2 mm has been found as the major factor in primary drying time, increasing the gravimetrical Kv up to 20 % for all the simulated chamber pressures. The effect of thermal conductivity was simulated using a polymer and aluminium vial replacing the standard glass vial of the same thickness. The polymer vial‘s decreased Kv value is 5.6 % at a low chamber pressure of 50 mTorr, and 12.2 % at 400 mTorr, which is in excellent agreement with the experiment. Using higher conductivity materials, for example, aluminium, only 3.7 % and 2.3 % Kv increase were computed for low and high chamber pressures respectively.
Ključne besede: freeze-drying, lyophilization speedup, vial heat conductivity, vial wall thickness, boundary element method
Objavljeno v DKUM: 16.04.2024; Ogledov: 167; Prenosov: 10
.pdf Celotno besedilo (1,88 MB)
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Measurements of material heat transfer properties : master study programme
Miha Donša, 2022, magistrsko delo

Opis: An experimental setup was created to observe temperature change at two points inside the experimental body. Such an experimental setup created data that was used as an anchor point of optimization that was coupled with numerical models to find unknown variables of heat conductivity and specific heat of the materials. Two numerical models were created. A 1D numerical model was created for possibilities of fast optimization ignoring the insulation and heat transfer through it. Such a model did not manage to describe the experimental setup accurately. Therefore, a 3D numerical model was created simulating the whole experimental setup and yielded much more promising results. Problems with the model were soon seen when experimental data was compared to the numerical solution where variables that were initially not taken into the account showed a much greater effect than first anticipated. Therefore, the 3D numerical model was adjusted to describe the experimental setup as accurately as possible. The experiment was done with two different materials. The materials were picked based on their heat conductivity (high and low). High heat conductivity material was easy to understand and to find a solution to it. With low conductivity material, some problems were quickly observed and as such created a lot of questions as to why and how to find the unknown variables of the material. It was then shown that the masses of the materials in the experiment and the length of the experiment played the most important role in the experiment and quickly explained why and how the experimental setup should be modified to obtain better results.
Ključne besede: heat transfer, material heat transfer properties, specific heat, heat conductivity, optimization, numerical simulation of heat transfer
Objavljeno v DKUM: 07.07.2022; Ogledov: 761; Prenosov: 45
.pdf Celotno besedilo (6,54 MB)

The combined analysis of phonon and electron heat transfer mechanism on thermal conductivity for nanofluids
Jurij Avsec, 2008, izvirni znanstveni članek

Opis: The paper features the mathematical model representing the analytical calculation of phonon and electron heat transfer analysis of thermal conductivity for nanofluids. The mathematical model was developed on the basis of statistical nanomechanics. We have made the detailed analysis of the influence of temperature dependence on thermal conductivity for nanofluids. On this basis are taken into account the influences such as formation of nanolayer around nanoparticles, the Brown motion of solid nanoparticles and influence of diffusive-ballistic heat transport. The analytical results obtained by statistical mechanics are compared with the experimental data and they show relatively good agreement.
Ključne besede: statistical nanomechanics, phonons, electron heat transfer, nanofluids, thermal conductivity, thermodynamic properties, mathematical model, statistical nanomechanics
Objavljeno v DKUM: 31.05.2012; Ogledov: 2578; Prenosov: 120
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