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Particles formation and particle design using supercritical fluids
Željko Knez, Eckhard Weidner, 2003, pregledni znanstveni članek

Opis: Major recent advances. Particle formation and design of solid particles and powdery composites with unique properties is at the moment a major developmentof supercritical fluids (synonymsČ dense gasses, dense fluids, highpressure) applications. This review will focus on recent advances and on fundamentals of these processes and their applications.
Ključne besede: chemical processing, high pressure technology, micronization, supercritical fluids, micro-particles, nano-particles, powder generation, crystallization, particles from gas saturated solutions
Objavljeno v DKUM: 01.06.2012; Ogledov: 3735; Prenosov: 108
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Experimental design of crystallization processes using Taguchi method
Miran Hvalec, Andreja Goršek, Peter Glavič, 2004, izvirni znanstveni članek

Opis: Crystallization has become one of the most important unit operation in the chemical industries. The need to reduce the time from product discovery to market introduction is an inherent concern. In order to achieve the prescribedproduct quality characteristics, the process of engineering experimentation has to be optimized. Therefore, an experimental design method for crystallization processes is presented in this paper. Initially, the standardized Taguchi method was used to plan a minimum number of experiments. After identifying the working levels of the design factors and the main performance characteristics of the product under study, the method can be successfully applied to the crystallization processes. The simultaneous variations of the main crystallization parameters and their interactions were investigated using orthogonal array technique. A statistical analysis of 'signal-to-noise' ratio was followed by performing a variance analysis. After developing some special criteria, which depend on performance objectives, the optimal levels of the design factors were determined. Crystallization of $KNO_3$ with desirable particle size as a performance characteristic was used to illustrate the design procedure. The effects of rotational frequency of the stirrer, linear cooling rate and added admixture on final particle size were studied. In order to keep the selected parameters constant during the experiment and to ensure reproduction of entire experiment the automated reaction calorimeter RC1 was used.
Ključne besede: crystallization, particle size, Taguchi method
Objavljeno v DKUM: 01.06.2012; Ogledov: 2511; Prenosov: 87
.pdf Celotno besedilo (701,22 KB)
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Magnetic water treatment for scale control in heating and alkaline conditions
Viljem Kozic, Anton Hamler, Irena Ban, Lucija Črepinšek-Lipuš, 2010, izvirni znanstveni članek

Opis: Magnetic water treatment (MWT), an alternative solution for scale control, is discussed with emphasis on the construction of the magnetic devices and the mechanism of MWT influence on the scale formation. Two applications in high-temperature and high-pH conditions are presented. The treatment noticeably reduced the scale thickness on the heating spiral and removed preciously precipitated scale from hot tap-water outlet pipe; on the walls in the zone with heated alkaline water, instead of hard scale, only thin, brittle coating was formed. The morphology analyses showed the acceleration of aragonite nucleation and raised formation of fine suspended particles.
Ključne besede: scale control, magnetic sater treatment, crystallization
Objavljeno v DKUM: 31.05.2012; Ogledov: 15380; Prenosov: 156
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