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Characterisation of a new dental alloy with high Au content
Rebeka Rudolf, Tjaša Zupančič Hartner, Ivan Anžel, Primož Mrvar, Jože Medved, Dragoslav Stamenković, 2007, izvirni znanstveni članek

Opis: The basis for developing a new dental alloy with high Au content is appropriate chemical composition and manufacturing technology. This new Au dental alloy is based on the ternary system of Au-Pt-Zn with a nominal composition of 88.5Au-8.7Pt-1.5Zn-0.5In-0.4Ir-0.3Rh. The alloy was melted and cast in a vacuum-induction melting furnace in Zlatarna Celje. Casting was followed with subsequent thermo-mechanical treatment (procedures of profile and polish milling, thermal treatment) and cutting-off strips to form a regular shape. The heat treatments of Au alloy samples were carried out in a tube furnace under different temperatures, and over different times. Testing of the new Au dental alloy included examining the initial cast, and the different heat treated conditions of the Au alloy. The optical properties of Au-dental alloy were investigated by means of spectrophotometric colourimetry. Finally the test of cytotoxicity of new Au based dental alloys using standard in vitro assays for testing the biocompatibility with establishing new, more sensitive, in vitro tests on cell lines was done.Osnovo razvoja nove dentalne zlitine z visoko vsebnostjo Au predstavljata pravilna določitev kemijske sestave in tehnologije izdelave. Nova dentalna zlitina temelji na ternarnem sistemu of Au-Pt-Zn z nominalno kemijsko sestavo 88,5Au-8,7Pt-1,5Zn-0,5In-0,4Ir-0,3Rh. Izdelava dentalne zlitine je potekala s pretaljevanjem zelo čistih komponent v vakuumski indukcijski peči v Zlatarni Celje. Temu je sledilo odlivanje taline v ustrezno formo, postopek termo-mehanske obdelave odlitka in razrez zlitine v ustrezno obliko. Toplotna obdelava je bila izvedena pri različnih temperaturah in za različne čase. Testiranje dentalne zlitine je vključevalo določitev lastnosti začetnega stanja in stanja po različnih toplotnih obdelavah. Optične lastnosti dentalne zlitine so bile raziskane s spektro-fotometrično kolorimetrijo. Na novi Au dentalni zlitini so bili narejeni še testi citotoksičnosti z uporabo standardain vitro analize za testiranje biokompatibilnosti z uvajanjem novih, bolj občutljivih in vitro testov na celični liniji.
Ključne besede: dental alloy, characterisation, microstructure, properties
Objavljeno: 31.05.2012; Ogledov: 1278; Prenosov: 31
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Characterization of Cu-Al-Ni melt-spun ribbons using a focussed ion beam (FIB)
Franc Zupanič, Elfride Unterweger, Albert C. Kneissl, Ivan Anžel, Gorazd Lojen, 2007, izvirni znanstveni članek

Opis: This work investigates the possibilities for applying a focussed ion beam (FIB) for the metallographic preparation and characterization of Cu-Al-Ni melt-spun ribbons. Two alloys were selected for this reason: CuAl13Ni4 and CuAl15Ni4. The microstructure of the first alloy was fully martensitic and the microstructure of the second consisted of two phases: martensite and ▫$\gamma_2$▫. It was discovered that with FIB-etching the microstructures of both alloys can be clearly revealed on polished cross-sections of the melt-spun ribbons, as well as on their wheel-side and air-side surfaces. However, better results were obtained when the etched surface was smoother, and finer details were visible when using smaller ion currents. In addition, a study was made into the influence of platinum deposition on the quality of 3D-cross sections. It was found that Pt-deposition is necessary when the edge of the trench should be straight and sharp, and the surface of the 3D cross-section smooth. However, in this case, the microstructure of the ribbons free surface cannot be seen.
Ključne besede: focussed ion beam, FIB, metallography, melt-spinning, shape memory alloy, Cu-Al-Ni
Objavljeno: 31.05.2012; Ogledov: 897; Prenosov: 18
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Modeling of impact toughness of cold formed material by genetic programming
Leo Gusel, Miran Brezočnik, 2006, izvirni znanstveni članek

Opis: In the paper, an approach completely different from the conventional methods for determination of accurate models for the change of properties of cold formed material, is presented. This approach is genetic programming (GP) method which is based on imitation of natural evolution of living organisms. The main characteristic of GP is its non-deterministic way of computing. No assumptions about the form and size of expressions were made in advance, but they were left to the self organization and intelligence of evolutionary process. First, copper alloy rods were cold drawn under different conditions and then impact toughness of cold drawn specimens was determined by Charpy tests. The values of independent variables (effective strain, coefficient of friction) influence the value of the dependent variable, impact toughness. On the basis of training data, different prediction models for impact toughness were developed by GP. Only the best models, gained by genetic programming were presented in the paper. Accuracy of the best models was proved with the testing data set. The comparison between deviation of genetic model results and regression model results concerning the experimental results has showed that genetic models are more precise and more varied then regression models.
Ključne besede: metal forming, genetic programming, evolutionary computing, impact toughness, copper alloy, modelling
Objavljeno: 30.05.2012; Ogledov: 1392; Prenosov: 72
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Dependence of material characteristics on lubrication in bulk forming process
Leo Gusel, 2009, objavljeni znanstveni prispevek na konferenci

Opis: In the paper the influence of coefficient of friction (lubricant) on different properties of cold formed material has been examined. Tensile tests, hardness measurements and electrical conductivity measurements were performed.In the frame of the experimental work the process of cold forward extrusion of a cylinder made from copper alloy was investigated. The specimens were extruded at four different lubricants coefficients of friction. The results have shown that use of different lubricators with different coefficients of friction can have effects on the material properties during and after cold forming process.
Ključne besede: lubrication, cold forming, copper alloy, mechanical properties
Objavljeno: 31.05.2012; Ogledov: 923; Prenosov: 10
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Microstructure of rapidly solidified Cu-Al-Ni shape memory alloy ribbons
Gorazd Lojen, Ivan Anžel, Albert C. Kneissl, Elfride Unterweger, Borut Kosec, Milan Bizjak, 2005, izvirni znanstveni članek

Opis: Cu-Al-Ni shape memory alloys (SMAs) are currently the only available high temperature SMAs, showing a good resistance against functional fatigue. In polycrystalline state, they are very brittle and exhibit, in general, only small reversible deformations. By melt spinning, thin Cu-Al-Ni ribbons can be manufactured directly from the melt. Appropriate casting parameters can ensurea single layer columnar structure with a fibre texture, which significantly increases the maximal reversible strain in longitudinal direction. Cu-Al-Ni ribbons, containing 13, 14 and 15 wt.% Al were cast by free jet melt spinning. Because of the alloys' low thermal conductivity, the cooling rate was surprisingly low - considering the crystal grain size - significantly below 103 K/s. Therefore, wide ribbons having a single layer columnar and (except the ribbons containing 13 wt.% Al) completely martensiticstructure could not be obtained. Regardless the chemical composition, the ribbons have a single layer columnar structure only if the thickness does not exceed approximately 50 m, otherwise the structure consists of at least two layers of equiaxed grains. In as-cast condition, only ribbons containing 13 wt.% Al seem to be completely martensitic. Heat treatments at temperatures up to 900 °C improved the structure of 13 and 14 wt.% Al ribbons. All ribbons exhibit one-way shape memory effect in as-cast condition. Heat-treated ribbons containing 13 wt.% Al exhibited two-way shape memory effect already after one bending and heating cycle.
Ključne besede: metallurgy, shape memory alloys, Cu-Al-Ni alloy, microstructure, melt spinning
Objavljeno: 01.06.2012; Ogledov: 1175; Prenosov: 74
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Response of monocyte-derived dendritic cells to rapidly solidified nickel-titanium ribbons with shape memory properties
Sergej Tomić, Rebeka Rudolf, Mihael Brunčko, Ivan Anžel, V. Savić, Miodrag Čolić, 2012, izvirni znanstveni članek

Opis: Ni-Ti Shape Memory Alloys (SMAs) have attracted considerable attention as biomaterials for medical devices. However, the biocompatibility of Ni-Ti SMAs is often unsatisfactory due to their poor surface structure. Here we prepared Rapidly Solidified (RS) Ni-Ti SMA ribbons by melt-spinning and their surface was characterised by Augerelectron spectroscopy, X-ray photoelectron spectrometry and scanning electron microscopy. The biocompatibility of the produced ribbons and their immunomodulatory properties were studied on human monocyte-derived dendritic cells (MoDCs). We showed that melt-spinning of Ni-Ti SMAs can form a thin homogenous oxide layer, which improves their corrosion resistance and subsequent toxicity to MoDCs. Ni-Ti RS ribbons stimulated the maturation of MoDCs, as detected by changes in the cells' morphology and increased expression of HLA-DR, CD86, CD40 and CD83 molecules. However, Ni-Ti RS ribbons enhanced the tolerogenic properties of immature MoDCs, which produced higher levels of IL-10 and IL-27, driving the differentiation of IL-10- and TGF-β-producing CD4+T cells. On the other hand, in the presence of lipopolysaccharide, an important pro-inflammatory biomolecule, Ni-Ti RS ribbons enhanced the allostimulatory and Th1 polarising capacity of MoDCs, whereas the production of Th2 and Th17 cytokines was down-regulated. In conclusion, Ni-Ti RS ribbons possess substantial immunomodulatory properties on MoDCs. These findings might be clinically relevant, because implanted Ni-Ti SMA devices can induce both desired and adverse effects on the immune system, depending on the microenvironmental stimuli.
Ključne besede: nickel-titanium alloy, biocompatibility, cytokines, immunomodulation, monocyte-derived dendritic cells
Objavljeno: 01.06.2012; Ogledov: 947; Prenosov: 203
.pdf Celotno besedilo (1,35 MB)
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In-situ monitoring of internal oxidation of dillute alloys
Mihael Brunčko, Ivan Anžel, Albert C. Kneissl, 2007, izvirni znanstveni članek

Opis: This paper presents a non-destructive measurement method that enables identification and characterization of phenomena during internal oxidation of metallic materials as well as monitoring the kinetics of internal oxidation using "in-situ" electrical resistance measurements. A special laboratory device, based on the unique measurement cell, for the electrical resistance measurements at high temperatures and the model for electrical resistance transformation into an instantaneous microstructure were developed. To accomplish this, the process of internal oxidation was divided into the sequence of the key partial reactions that were presented in the model as the parallel andžor serial connected time variable resistors in the electrical circuit. The validity of the transformation model was experimentally confirmedby internal oxidation of Ag-Sn (2 at.% Sn) alloy at different oxidation temperatures in air atmosphere. The comparison of the results obtained by "in-situ" electrical resistance measurements with those obtained by metallographic analysis and Wagnerćs theory shows that the novel method presents a more effective tool for monitoring of internal oxidation kinetics. The method identifies also the microstructural defects and their influences onthe kinetics of internal oxidation.
Ključne besede: metallurgy, Ag-Sn alloy, internal oxidation, electrical resistance
Objavljeno: 01.06.2012; Ogledov: 891; Prenosov: 22
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Monitoring of directional solidification with simultaneous measurements of electrical resistance and temperature
Mihael Brunčko, Ivan Anžel, Alojz Križman, 2003, izvirni znanstveni članek

Opis: WE present the efficiency of simultaneous electrical resistance and temperature (ERT) measurements for monitoring the position, X, and the growth rate, V, of the solidification front during the directional solidification of alloys. On alaboratory device for directional solidification (Bridgman-type furnace), theeutectic Pb-Sn alloy was solidified at five different pulling rates, VP, with a constant imposed temperature gradient, GP. During directional solidification, the electrical resistance and the temperature changes were measured simultaneously in the experimental samples. The results of the experiments show that simultaneous measurement of ERT enables not only the determination of the average growth rate, V, during directional solidificationbut also its fluctuation over the total measurement length of the sample.
Ključne besede: metallurgy, Pb-Sn alloy, directional solidification, electrical resistance measurements, temperature measurements
Objavljeno: 01.06.2012; Ogledov: 1028; Prenosov: 68
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