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1.
Use of AFM force spectroscopy for assessment of polymer response to conditions similar to the wound, during healing
Uroš Maver, Tina Maver, Andrej Žnidaršič, Zdenka Peršin, Miran Gaberšček, Karin Stana-Kleinschek, 2011, izvirni znanstveni članek

Opis: Force spectroscopy is a very promising technique for the evaluation of interactions within different environments. Knowledge about them is especially important during the design and preparation of those modern wound dressings in contact with a changing wound-environment over a prolonged time. Such exposure can cause a drastic decrease in the materialćs mechanical performance, and can lead to degradation, thus lowering the success of any healing process. Our study tries to establish a model system, which would enable us to assess the applicability of the mentioned technique for the evaluation of any interaction changes between polymer molecules and a chosen surface, after exposure to different environments. Our proposed experimental setup consists of two representative polymers, a model silicon surface, and two solutions of various pHs and ionic strengths, respectively. Within the chosen range of parameters, we are confident that we can prove the usefulness of force spectroscopy for further research into polymer suitability, for the development of novel wound dressings.
Ključne besede: force spectroscopy, AFM, wound dressings, polymer materials, model system
Objavljeno: 01.06.2012; Ogledov: 1058; Prenosov: 49
.pdf Celotno besedilo (316,48 KB)
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2.
Binding silver nano-particles onto viscose non-woven using different commercial sol-gel procedures
Tanja Pivec, Zdenka Peršin, Silvo Hribernik, Tina Maver, Mitja Kolar, Karin Stana-Kleinschek, 2012, izvirni znanstveni članek

Opis: The paper presents possible solution of Ag binding using commercial sol-gel systems which enable its low release into a wound, providing a good antimicrobial effect on those bacterial cultures that are most likely present in the wound. The influence of different sol-gel systems on the hydrophilic properties of carrier materials and the level of released silver has been studied. The results showed that sol-gel as binding-systems could provide proper hydrophilic properties of material, whilst binding silver strongly enough providing at the same time excellent antimicrobial activity of the treated viscose meterials.
Ključne besede: silver nano-particles, sol-gel, viscose non-woven, silver release, hydrophilicity, antimicrobial properties
Objavljeno: 01.06.2012; Ogledov: 1917; Prenosov: 38
.pdf Celotno besedilo (235,88 KB)
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Modification of non-woven cellulose for medical applications using non-equlibrium gassious plasma
Karin Stana-Kleinschek, Zdenka Peršin, Tina Maver, 2011, izvirni znanstveni članek

Opis: This paper presents the use of a non-equilibrium gaseous plasma technique for the activation of regenerated non-woven cellulose, as used in the preparation of wound-dressing materials. Plasma technology provides surface modification according to the required quality in terms of speed, homogeneity, process stability, and efficiency. In this study the non-woven cellulose was exposed to oxygen plasma (O2) in order to acquire the natural polymer's super-hydrophilicity which, among others, defines the materials' usability forwound-dressing. The influence of the plasma parameters on the material's hydrophilicity was studied; and the optimal plasma conditions defined. Combinations of different experimental techniques (contact angle, water retention value, and moisture content) were studied and correlated with the mechanical properties, as a function of plasma modification. The specific adsorption capacity of the non-woven cellulose using oxygen plasma treatment was achieved. In the next step, this material with increased hydrophilicity and improved mechanical properties will be used in the preparation of multilayered wound-dressing materials for specific functionalities (incorporation of drugs, specific functional properties).
Ključne besede: plasma, oxygen, regenerated non-woven cellulose, super-hydrophilicity, mechanical properties
Objavljeno: 10.07.2015; Ogledov: 424; Prenosov: 36
.pdf Celotno besedilo (101,91 KB)
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5.
Functionalization of AFM tips for use in force spectroscopy between polymers and model surfaces
Tina Maver, Karin Stana-Kleinschek, Zdenka Peršin, Uroš Maver, 2011, izvirni znanstveni članek

Opis: The following work presents the use of two different methods for the attachment of different functional groups onto the AFM tip surface. Such functionalized tips then allow for further binding of molecules with different origins and natures, thus allowing for use when measuring forces, and the extent of interactions appearing between two model surfaces and in real systems. Force spectroscopy, in combination with chemical force microscopy (CFM), as used in this study, exhibits great potential for chemical sensing in the field of polymer sciences. In modern wound treatment, it is very important to know the type and ranges of interactions between different polymer materials, which are mostly crucial components of the dressings. Precise measurement of these interactions would help to choose those materials that fit together without the use of additional chemical modifications on their surfaces. Such modifications are often the cause of unpredictable complications during the course of wound healing. This same method could also be used for interaction evaluation between chosen polymer materials with biological macromolecules, which appear within the wound during the healing process. Such in vitro testing could be of great help when optimal wound dressing materials need to be chosen in order to alleviate a patient s suffering after application. Scanning electron and atomic force microscopies were used in order to prove the effectiveness and applicability of the used functionalization procedures.
Ključne besede: atomic force microscopy, chemical force microscopy, force spectroscopy, functionalization of AFM tips
Objavljeno: 10.07.2015; Ogledov: 770; Prenosov: 57
.pdf Celotno besedilo (550,85 KB)
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