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DSC/TG of Al-based alloyed powders for p/m applications
Borivoj Šuštaršič, Jože Medved, Srečko Glodež, Marko Šori, Albert Korošec, 2014, izvirni znanstveni članek

Opis: Al-based alloyed powders, appropriate for the sintering procedure (powder metallurgy, P/M) contain the alloying elements with a high solid solubility in Al, enabling reaction and liquid-phase sintering. They are surface oxidised because of a high affinity of Al to oxygen. Besides, this type of powders contains a polymeric lubricant (wax), which reduces the friction on die walls during automatic die compaction into the final compact shape of a product. This lubricant has to be removed slowly during the first stage of sintering in order to prevent deformations and cracking of the product. Consequently, its sintering is very complex. Generally, these powders are sintered in pure nitrogen with a low dew point. The optimum sintering conditions are generally determined on the basis of light and scanning electron microscopy. The investigation can also be completed very successively with differential scanning calorimetry and thermo gravimetry. The first one allows an insight into the endo- and exothermic reactions, taking place during the heating and cooling of a compacted metal powder, and the second one allows an insight into the processes, connected with the mass loss (a reduction, a lubricant removal, etc.) or mass increase (an oxidation). The DSC/TG of three commercial Al-based alloyed powders was performed in the frame of our investigations. The results were compared with the theoretical thermodynamic-based calculations and the optimum sintering conditions were proposed.
Ključne besede: aluminium powders, sintering, differential scanning calorimetry and thermo gravimetry
Objavljeno v DKUM: 15.03.2017; Ogledov: 1384; Prenosov: 139
Celotno besedilo (319,52 KB)
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Characterisation of a new dental alloy with high Au content
Rebeka Rudolf, Tjaša Zupančič Hartner, Ivan Anžel, Primož Mrvar, Jože Medved, Dragoslav Stamenković, 2007, izvirni znanstveni članek

Opis: The basis for developing a new dental alloy with high Au content is appropriate chemical composition and manufacturing technology. This new Au dental alloy is based on the ternary system of Au-Pt-Zn with a nominal composition of 88.5Au-8.7Pt-1.5Zn-0.5In-0.4Ir-0.3Rh. The alloy was melted and cast in a vacuum-induction melting furnace in Zlatarna Celje. Casting was followed with subsequent thermo-mechanical treatment (procedures of profile and polish milling, thermal treatment) and cutting-off strips to form a regular shape. The heat treatments of Au alloy samples were carried out in a tube furnace under different temperatures, and over different times. Testing of the new Au dental alloy included examining the initial cast, and the different heat treated conditions of the Au alloy. The optical properties of Au-dental alloy were investigated by means of spectrophotometric colourimetry. Finally the test of cytotoxicity of new Au based dental alloys using standard in vitro assays for testing the biocompatibility with establishing new, more sensitive, in vitro tests on cell lines was done.Osnovo razvoja nove dentalne zlitine z visoko vsebnostjo Au predstavljata pravilna določitev kemijske sestave in tehnologije izdelave. Nova dentalna zlitina temelji na ternarnem sistemu of Au-Pt-Zn z nominalno kemijsko sestavo 88,5Au-8,7Pt-1,5Zn-0,5In-0,4Ir-0,3Rh. Izdelava dentalne zlitine je potekala s pretaljevanjem zelo čistih komponent v vakuumski indukcijski peči v Zlatarni Celje. Temu je sledilo odlivanje taline v ustrezno formo, postopek termo-mehanske obdelave odlitka in razrez zlitine v ustrezno obliko. Toplotna obdelava je bila izvedena pri različnih temperaturah in za različne čase. Testiranje dentalne zlitine je vključevalo določitev lastnosti začetnega stanja in stanja po različnih toplotnih obdelavah. Optične lastnosti dentalne zlitine so bile raziskane s spektro-fotometrično kolorimetrijo. Na novi Au dentalni zlitini so bili narejeni še testi citotoksičnosti z uporabo standardain vitro analize za testiranje biokompatibilnosti z uvajanjem novih, bolj občutljivih in vitro testov na celični liniji.
Ključne besede: dental alloy, characterisation, microstructure, properties
Objavljeno v DKUM: 31.05.2012; Ogledov: 2174; Prenosov: 60
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