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Abstract: Titanium and its alloys, as well as stainless steel, are commonly used materials for implants in the human body due to their excellent biocompatibility, corrosion resistance, and mechanical properties. However, the long-term performance of these materials in the oral cavity can be affected by the complex oral environment, including the ingestion of food, beverages, and oral hygiene products, leading to the presence of various ions, pH fluctuations, and inflammatory processes. In this study, the corrosion properties of two biocompatible materials, Ti6Al4V and AISI 316L stainless steel, are investigated under varying oral inflammatory conditions. Using potentiodynamic polarization, electrochemical impedance spectroscopy (EIS), SEM, and EDS analysis, the corrosion behaviour of both materials was analysed in environments simulating mild and severe inflammation. Results indicate that Ti6Al4V exhibits superior corrosion resistance at low H2O2 concentrations mimicking mild inflammation, with significantly lower corrosion rates compared to AISI 316L. However, at higher H2O2 concentrations, which correspond to severe inflammation, AISI 316L shows better resistance despite its susceptibility to pitting corrosion. Both alloys show reduced passivation after 72 h, with corrosion products accumulating on the surface after 96 h, contributing to repassivation. These results emphasise the need for individualized material selection in dental applications based on a patient’s susceptibility to oral inflammation.
Keywords: corrosion, EIS, inflammatory conditions, titanium, stainless steel, dental materials
Published in DKUM: 19.05.2025; Views: 0; Downloads: 0
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Abstract: Štore Steel Ltd. is one of the biggest flat spring steel producers in Europe. The main motive for this study was to study the influences of non-metallic inclusions on mechanical properties obtained by tensile testing. From January 2016 to December 2021, all available tensile strength data (472 cases–472 test pieces) of 17 low alloy steel grades, which were ordered and used by the final user in rolled condition, were gathered. Based on the geometry of rolled bars, selected chemical composition, and average size of worst fields non-metallic inclusions (sulfur, silicate, aluminium and globular oxides), determined based on ASTM E45, several models for tensile strength, yield strength, percentage elongation, and percentage reduction area were obtained using linear regression and genetic programming. Based on modeling results in the period from January 2022 to April 2022, five successively cast batches of 30MnVS6 were produced with a statistically significant reduction of content of silicon (t-test, p < 0.05). The content of silicate type of inclusions, yield, and tensile strength also changed statistically significantly (t-test, p < 0.05). The average yield and tensile strength increased from 458.5 MPa to 525.4 MPa and from 672.7 MPa to 754.0 MPa, respectively. It is necessary to emphasize that there were no statistically significant changes in other monitored parameters.
Keywords: mechanical properties, tensile test, tensile strength, yield strength, percentage elongation, percentage reduction area, low alloy steel, modeling, linear regression, genetic programming, industrial study, steel making, optimization
Published in DKUM: 24.03.2025; Views: 0; Downloads: 2
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Abstract: There is a need to develop new construction materials with improved mechanical performance and durability that are low-priced and have environmental benefits at the same time. This paper focuses on the rheological, mechanical, morphological, and durability properties of synthetic and steel fiber reinforced self-compacting concrete (SCC) containing 5–15% metakaolin (M) by mass as a green replacement for Portland cement. Testing of the fresh mixes included a slump-flow test, density, and porosity tests. Mechanical properties were determined through compression and flexural strength. A rapid chloride penetrability test (RCPT) and the chloride migration coefficient were used to assess the durability of the samples. A scanning electron microscope (SEM) with energy dispersion spectrometry (EDS) was used to study the concrete microstructure and the interfacial transition zone (ITZ). The results show that a combination of metakaolin and hybrid fibers has a negative effect on the flowability of SCC. In contrast, the inclusion of M and hybrid fibers has a positive effect on the compressive and flexural strength of SCC. The fracture of SCC samples without fibers was brittle and sudden, unlike the fiber-reinforced SCC samples, which could still transfer a considerable load with increasing crack mouth opening deflection. Overall, the chloride migration coefficients were reduced by up to 71% compared to the control mix. The chloride reduction is consistent with the resulting compact concrete microstructure, which exhibits a strong bond between fibers and the concrete matrix.
Keywords: self-compacting concrete, synthetic and steel fibers, metakaolin, rheology, mechanical properties, chloride penetration, SEM-EDS
Published in DKUM: 12.03.2025; Views: 0; Downloads: 3
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Abstract: Heat-affected zones (HAZs) in real welds are usually quite narrow, and consequently most standard mechanical tests are difficult or even impossible. Therefore, simulated microstructures are often used for mechanical tests. However, the most often used weld thermal cycle simulator produces only a few millimeters wide area of simulated microstructure in the middle of specimens. Consequently, these kind of simulated specimen are not suitable for standard tensile tests, and even for Charpy impact tests, the simulated area can be too narrow. Therefore, to investigate the mechanical properties of a fine-grain heat-affected zone in 18CrNiMo7-6 steel, two methods were used for simulation of as-welded microstructures: (a) a weld thermal cycle simulator, and (b) as an alternative, though not yet verified option, austenitizing in a laboratory furnace + water quenching. The microstructures were compared and mechanical properties investigated. The grain sizes of the simulated specimens were 10.9 μm (water-quenched) and 12.6 μm (simulator), whereby the deviations from the real weld were less than 10%. Both types of simulated specimen were used for hardness measurement, Charpy impact tests, and fatigue tests. Water-quenched specimens were large enough to enable standard tensile testing. A hardness of 425 HV, yield strength Rp02 = 1121 MPa, tensile strength Rm = 1475 MPa, impact energy KV = 73.11 J, and crack propagation threshold ΔKthR = 4.33 MPa m0.5 were obtained with the water quenched specimens, and 419 HV, KV = 101.49 J, and ΔKthR = 3.4 MPa m0.5 with the specimens prepared with the simulator. Comparison of the results confirmed that the annealed and quenched specimens were suitable for mechanical tests of FG HAZs, even for standard tensile tests. Due to the use of simulated test specimens, the mechanical properties determined can be linked to the FG HAZ microstructure in 18CrNiMo7-6 steel.
Keywords: weld joint, fine-grained HAZ, simulation of microstructure, hardness, impact toughness, tensile properties, fatigue crack growth, 18CrNiMo7-6 steel
Published in DKUM: 05.12.2024; Views: 0; Downloads: 8
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Abstract: AISI 316L austenitic stainless steel is utilized in various processing industries, due to its abrasion resistance, corrosion resistance, and excellent properties over a wide temperature range. The physical and mechanical properties of a material change during the manufacturing process and plastic deformation, e.g., bending. During the combined tensile and bending loading of a structural component, the stress state changes due to the residual stresses and the loading range. To characterize the component’s stress state, the billet was bent to induce residual stress, but a phase transformation to martensite also occurred. The bent billet was subjected to combined tensile–bending and fatigue loading. The experimentally measured the load vs. displacement of the bent billet was compared with the numerical simulations. The results showed that during fatigue loading of the bent billet, both the initial stress state at the critical point and the stress state during the dynamic loading itself must be considered. Analysis was demonstrated only for one single critical point on the surface of the bent billet. The residual stresses due to the phase transformation of austenite to martensite affected the range and ratio of stress. The model for the stress–strain behaviour of the material was established by comparing the experimentally and numerically obtained load vs. displacement curves. Based on the description of the stress–strain behaviour of the pre-deformed material, guidelines have been provided for reducing residual tensile stresses in pre-deformed structural components.
Keywords: metastable austenitic stainless steel, fatigue, residual stress, phase transformation
Published in DKUM: 28.11.2024; Views: 0; Downloads: 6
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