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1.
The influence of enzymatic treatment on wool fibre properties using PEG-modified proteases
Suzana Jus, Marc Schroeder, Georg M. Gübitz, Elisabeth Heine, Vanja Kokol, 2007, original scientific article

Abstract: The main contribution of the presented work was to introduce the use of proteases modified with the soluble polymer polyethylene glycol (PEG) in the bio-finishing process of wool fibres, to target enzyme action to the outerparts of wool fibres, i.e. to avoid the diffusion and consequent destroying of the inner parts of the wool fibre structure, in the case of native proteases using. Different proteolytic enzymes from Bacillus lentus and Bacillus subtilis in native and PEG-modified forms were investigated and their influence on the modification of wool fibres morphology surface, chemical structure, as well as the hydrolysis of wool proteins, the physico-mechanical properties, and the sorption properties of 1:2 metal complex dye during dyeing were studied. SEM images of wool fibres confirmed smoother and cleaner fibre surfaces without fibre damages using PEG-modified proteases. Modified enzyme products have a benefit effect on the wool fibres felting behaviours (14%) in the case when PEG-modified B. lentus is used, without markedly fibre damage expressed by tensile strength and weight loss ofthe fibre. Meanwhile the dye exhaustion showed slower but comparable level of dye uptake at the end of the dyeing.
Keywords: volnena vlakna, proteolitski encimi, encimske modifikacije, sorpcija barve, morfologija vlaken, wool fibres, proteolytic enzymes, enzyme modification, felting, dye sorption, protein hydrolysis, XPS-analysis, fibre morphology
Published: 01.06.2012; Views: 1664; Downloads: 64
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2.
Disociacijsko-adsorpcijske značilnosti PA 6 vlaken z uporabo titracijskih metod
Lidija Fras Zemljič, Karin Stana-Kleinschek, Simona Strnad, Volker Ribitsch, 2001, original scientific article

Abstract: Različni postopki obdelave orientiranih polimerov lahko povzročajo spremembe nadmolekulske strukture in tako spreminjajo njihovo morfologijo. S strukturnimi spremembami vlaken se spreminjajo tudi površinske lastnosti, ki so bistvenega pomena za njihov adsorpcijski značaj. Osredotočili smo se na raziskave disociacijsko-adsorpcijskih značilnosti strukturno modificiranih tekstilnih vlaken, ki smo jih opredelili s titracijskimi metodami. Uporaba različnih titracijskih metod za spremljanje disociacijsko-adsorpcijskih sposobnosti tekstilnih vlaken v polarnem mediju predstavlja novost na področju raziskav vlaken. Namen prispevka je ocenitev količine značilnih disociacijskih skupin na PA 6 vlaknih, strukturno modificiranih z različnimi postopki visokotemperaturne obdelave in z obdelavo v raztopini fenola, v primerjavi z ostalimi fizikalno-kemijskimi lastnostmi vlaken (molekulska masa, pokazatelji nadmolekulske strukture vlaken, jodovo adsorpcijsko število ...). Na podlagi rezultatov smo želeli ugotoviti vpliv strukturnih modifikacij na disociacijsko-adsorpcijske značilnosti vlaken in posledično na njihovo reaktivnost. Spoznanja o številu in dostopnosti reaktivnih skupin vlaken vodijo k razjasnitvi reakcijskega mehanizma v procesih predobdelave, obdelave in ostalih proizvodnih procesih, hkrati pa lahko dajejo pomembne informacije o spremembah, ki se dogajajo pri degradaciji vlaken.
Keywords: orientirani polimeri, nadmolekulska struktura, morfologija vlaken, strukturno modificirana tekstilna vlakna, titracijske metode, reaktivne skupine, reakcijski mehanizem
Published: 31.08.2017; Views: 334; Downloads: 41
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