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1.
Experimental and mathematical investigation of anaerobic granulate density via settling velocity
Aljaž Klasinc, Gregor Drago Zupančič, Matjaž Hriberšek, Aleš Hribernik, Aleksandra Lobnik, Matej Zadravec, 2022, original scientific article

Abstract: The objective of this study was to determine the density of anaerobic granules on different heights of a full-scale Upflow Anaerobic Sludge Bed reactor. The density was defined through the settling velocities of anaerobic granules, measured in a full-scale Upflow Anaerobic Sludge Bed reactor. In this study, granular density was calculated with the measured settling velocities and developed mathematical model. The developed mathematical model is based on the Stokes model. In the experiment, granules were taken from different heights of an Upflow Anaerobic Sludge Bed reactor, from 0.6 to 7.6 m. The granules’ diameters varied between 1 and 5 mm. The granules were taken from six different heights through the reactor. The settling velocity of the active granules (with gas in the granule pore and on the surface of the granule) was measured first. After the active granules’ settling velocity measurement, the granules were placed in a vortex to obtain degassed granules (granules without any gas in the pores or on the surface), for which the settling velocities were also measured later. It is shown that granules’ densities at different heights are independent of the reactor height.
Keywords: Upflow Anaerobic Sludge Bed reactor, microstructure, anaerobic granular sludge, settling velocity, density
Published in DKUM: 26.03.2025; Views: 0; Downloads: 5
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2.
Microstructure and indentation properties of single-roll and twin-roll casting of a quasicrystal-forming Al-Mn-Cu-Be alloy
Franc Zupanič, Matjaž Macerl, Toshio Haga, Tonica Bončina, 2022, original scientific article

Abstract: In this investigation, strips of an experimental Al-Mn-Cu-Be alloy were manufactured by high-speed single-roll and twin-roll casting to stimulate the formation of a quasicrystalline phase during solidification. The strips were characterised by light microscopy, scanning and transmission electron microscopy, microchemical analysis, and X-ray diffraction. Indentation testing was used to determine the mechanical responses of the strips in different areas. A smooth surface was achieved on both sides of the twin-roll-cast strip, while the free surface of the single-roll-cast strip was rough. The microstructures in both strips consisted of an Al-rich solid solution matrix embedding several intermetallic phases Θ-Al2Cu, Be4Al (Mn, Cu), Al15Mn3Be2 and icosahedral quasicrystalline phase (IQC). The microstructure of the single-roll-cast strip was more uniform than that of the twin-roll-cast strip. Coarse Al15Mn3Be2 particles appeared in both alloys, especially at the centre of the twinroll strip. These coarse particles adversely affected the strength and ductility. Nevertheless, both casting methods provided high-cooling rates, enabling the formation of metastable phases, such as quasicrystals. However, improvements in alloy composition and casting procedure are required to obtain enhanced microstructures and properties.
Keywords: single-roll casting, twin roll casting, microstructure, quasicrystal, hardness, aluminium, characterisation
Published in DKUM: 24.03.2025; Views: 0; Downloads: 4
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3.
Oxidation behaviour of microstructurally highly metastable Ag-La alloy
Andraž Jug, Mihael Brunčko, Rebeka Rudolf, Ivan Anžel, 2022, original scientific article

Abstract: A new silver-based alloy with 2 wt.% of lanthanum (La) was studied as a potential candidate for electric contact material. The alloy was prepared by rapid solidification, performed by the melt spinning technique. Microstructural examination of the rapidly solidified ribbons revealed very fine grains of αAg and intermetallic Ag5La particles, which appear in the volume of the grains, as well as on the grain boundaries. Rapid solidification enabled high microstructural refinement and provided a suitable starting microstructure for the subsequent internal oxidation, resulting in fine submicronsized La2O3 oxide nanoparticle formation throughout the volume of the silver matrix (αAg). The resulting nanostructured Ag-La2O3 microstructure was characterised by high-resolution FESEM and STEM, both equipped with EDX. High-temperature internal oxidation of the rapidly solidified ribbons essentially changed the microstructure. Mostly homogeneously dispersed nano-sized La2O3 were formed within the grains, as well as on the grain boundaries. Three mechanisms of internal oxidation were identified: (i) the oxidation of La from the solid solution; (ii) partial dissolution of finer Ag5La particles before the internal oxidation front and oxidation of La from the solid solution; and (iii) direct oxidation of coarser Ag5La intermetallic particles.
Keywords: Ag-La alloy, rapid solidification, metastable microstructure, internal oxidation, characterisation, formation mechanism
Published in DKUM: 20.03.2025; Views: 0; Downloads: 1
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4.
Simulation and mechanical properties of fine-grained heat-affected zone microstructure in 18CrNiMo7-6 steel
Tomaž Vuherer, Fidan Smaili, Edvard Bjelajac, Mirza Manjgo, Gorazd Lojen, 2022, original scientific article

Abstract: Heat-affected zones (HAZs) in real welds are usually quite narrow, and consequently most standard mechanical tests are difficult or even impossible. Therefore, simulated microstructures are often used for mechanical tests. However, the most often used weld thermal cycle simulator produces only a few millimeters wide area of simulated microstructure in the middle of specimens. Consequently, these kind of simulated specimen are not suitable for standard tensile tests, and even for Charpy impact tests, the simulated area can be too narrow. Therefore, to investigate the mechanical properties of a fine-grain heat-affected zone in 18CrNiMo7-6 steel, two methods were used for simulation of as-welded microstructures: (a) a weld thermal cycle simulator, and (b) as an alternative, though not yet verified option, austenitizing in a laboratory furnace + water quenching. The microstructures were compared and mechanical properties investigated. The grain sizes of the simulated specimens were 10.9 μm (water-quenched) and 12.6 μm (simulator), whereby the deviations from the real weld were less than 10%. Both types of simulated specimen were used for hardness measurement, Charpy impact tests, and fatigue tests. Water-quenched specimens were large enough to enable standard tensile testing. A hardness of 425 HV, yield strength Rp02 = 1121 MPa, tensile strength Rm = 1475 MPa, impact energy KV = 73.11 J, and crack propagation threshold ΔKthR = 4.33 MPa m0.5 were obtained with the water quenched specimens, and 419 HV, KV = 101.49 J, and ΔKthR = 3.4 MPa m0.5 with the specimens prepared with the simulator. Comparison of the results confirmed that the annealed and quenched specimens were suitable for mechanical tests of FG HAZs, even for standard tensile tests. Due to the use of simulated test specimens, the mechanical properties determined can be linked to the FG HAZ microstructure in 18CrNiMo7-6 steel.
Keywords: weld joint, fine-grained HAZ, simulation of microstructure, hardness, impact toughness, tensile properties, fatigue crack growth, 18CrNiMo7-6 steel
Published in DKUM: 05.12.2024; Views: 0; Downloads: 8
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5.
The influence of the rolling direction on the mechanical properties of the Al-Alloy EN AW-5454-D
Matjaž Balant, Tomaž Vuherer, Peter Majerič, Rebeka Rudolf, 2024, original scientific article

Abstract: A complementary characterisation of the Al-alloy EN AW-5454 was carried out, intended for obtaining the laser hybrid welding parameters of subassemblies in the automotive industry. The investigation included a microstructural examination and the determination of the alloy’s properties using several analytical methods (HV5 hardness measurement, tensile test, Charpy impact toughness, fracture mechanics analysis). Samples were prepared in the longitudinal and transverse directions of a cold-rolled sheet of EN AW-5454 with thicknesses of 3.5 mm and 4 mm. The measured hardness on the thinner sheet was 5% higher than on the thicker sheet. The tensile and yield strength were nominal, while the elongations were smaller by 2.2–3.2% for the longitudinal samples and by 2.7–13.7% for the transverse samples. The smaller deviations from the nominal values are for the thinner sheet metal. A precise topographical analysis showed the brittle fractures of the samples. The Charpy impact toughness results on the thicker plate showed a 20% greater work needed to break it in the longitudinal direction than in the transverse direction. With the thinner sheet metal, 40% greater work was needed. SEM (scanning electron microscope) analysis has shown that the intermetallic Al6(Mn,Fe) particles in the longitudinal samples were mostly intact, with evidence of tough areas on the upper part of the fracture, indicating a better toughness than the specimens in the transverse direction. More crushed intermetallic particles were observed at the fractures of the transverse samples, and their distribution appeared to be more oriented in the direction of rolling. Fracture mechanics SENB (single edge notch bending) tests and their analysis showed that the resistance of the material to crack propagation in the longitudinal sample was about 50% greater than that in the transverse sample. SEM analysis of the fractures showed that the state of the intermetallic particles in the fracture mechanics testing and the fracture mechanism differed from the one in the Charpy fractures.
Keywords: Al-alloy EN AW-5454, characterisation, microstructure, properties
Published in DKUM: 02.12.2024; Views: 0; Downloads: 6
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ǂThe ǂcorrosion resistance of dental Ti6Al4V with differing microstructures in oral environments
Mirjam Bajt Leban, Tadeja Kosec, Matjaž Finšgar, 2023, original scientific article

Abstract: The impact of the microstructural properties of a Ti6Al4V alloy on its electrochemical properties, as well as the effect of the α- and β-phases present within it, is still unclear. With the introduction of new, emerging technologies, such as selective laser melting and post heat treatments, the effect of the microstructure on an alloy's corrosion properties has become increasingly interesting from a scientific perspective. When these alloys are produced through different methods, despite an identical chemical composition they have diverse microstructures, and consequently display varying resistance to corrosion. In the present research study, Ti–6Al–4V alloy specimens produced by three different processes, leading to the formation of three different microstructures were investigated: heat treated specimen fabricated by selective laser melting, wrought and cast specimens. The impact of the microstructure of these alloys when immersed in artificial saliva was studied through the use of various electrochemical techniques, by microscopical examinations, and time-of-flight secondary ion mass spectrometry. Corrosion properties were investigated by the measurement of open circuit potential, linear polarization, and potentiodynamic curve measurements followed by microscopical examinations, and time-of-flight secondary ion mass spectrometry examination was conducted to reveal spatial distribution of alloying species on oxide film. It was found that the difference between specimens containing an α+β microstructure was small and not dependent on the aspect ratio of the β-phase, alloy grain size, and vanadium partitioning coefficient, but rather on the size, shape, and content of this phase.
Keywords: Ti6Al4V, dental alloy, microstructure, corrosion resistance, heat treatment, ToF-SIMS
Published in DKUM: 07.05.2024; Views: 198; Downloads: 15
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