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Abstract: This study investigated the thermomechanical behavior of 4D-printed polylactic acid (PLA), focusing on its response to varying temperatures and strain rates in a wide range below the glass transition temperature (Tg). The material was characterized using tension, compression, and dynamic mechanical thermal analysis (DMTA), confirming PLA’s strong dependency on strain rate and temperature. The glass transition temperature of 4D-printed PLA was determined to be 65 °C using a thermal analysis (DMTA). The elastic modulus changed from 1045.7 MPa in the glassy phase to 1.2 MPa in the rubber phase, showing the great shape memory potential of 4D-printed PLA. The filament tension tests revealed that the material’s yield stress strongly depended on the strain rate at room temperature, with values ranging from 56 MPa to 43 MPA as the strain rate decreased. Using a commercial FDM Ultimaker printer, cylindrical compression samples were 3D-printed and then characterized under thermo-mechanical conditions. Thermo-mechanical compression tests were conducted at strain rates ranging from 0.0001 s−1 to 0.1 s−1 and at temperatures below the glass transition temperature (Tg) at 25, 37, and 50 °C. The conducted experimental tests showed that the material had distinct yield stress, strain softening, and strain hardening at very large deformations. Clear strain rate dependence was observed, particularly at quasi-static rates, with the temperature and strain rate significantly influencing PLA’s mechanical properties, including yield stress. Yield stress values varied from 110 MPa at room temperature with a strain rate of 0.1 s−1 to 42 MPa at 50 °C with a strain rate of 0.0001 s−1. This study also included thermo-mechanical adiabatic tests, which revealed that higher strain rates of 0.01 s−1 and 0.1 s−1 led to self-heating due to non-dissipated generated heat. This internal heating caused additional softening at higher strain rates and lower stress values. Thermal imaging revealed temperature increases of 15 °C and 18 °C for strain rates of 0.01 s−1 and 0.1 s−1, respectively.
Keywords: smart materials, shape memory polymer, 3D printing, 4D printing, thermo-mechanical experiments
Published in DKUM: 29.05.2024; Views: 248; Downloads: 22
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Abstract: V magistrskem delu je predstavljen postopek trdnostne analize ploščnega tipa toplotnega izmenjevalca. Da lahko izvedemo numerični preračun po metodi končnih elementov (MKE), je potrebno pridobiti 3D model toplotnega izmenjevalca. Model ploščnega tipa toplotnega izmenjevalca je bil pridobljen s pomočjo skeniranja oz. 3D računalniške tomografije. Na podlagi pridobljene geometrije s skeniranjem je bilo potrebno le-to ustrezno popraviti, da smo jo lahko nato uporabili za numerični preračun (numerični 3D model). Geometrija je bila parameterizirana, kar nam je omogočilo izvedbo parametričnih simulacij (spremljanje različnih odzivov glede na vhodno geometrijo). V numeričnem preračunu smo se ukvarjali z obremenitvenimi primeri prelotanih in neprelotanih mest v toplotnem izmenjevalcu ter posledično z različnimi napetostno deformacijskimi stanji in njihovim vplivom na pričakovano življenjsko dobo toplotnega izmenjevalca. Numerični preračuni (MKE) so bili izvedeni v programskem paketu Ansys Workbench, pri čemer smo pridobljene rezultate analizirali ter ustrezno karakterizirali odzive glede na predhodno določene obremenitvene primere.
Keywords: toplotni izmenjevalec, modeliranje, trdnostna analiza, numerična simulacija, MKE
Published in DKUM: 24.08.2023; Views: 589; Downloads: 0
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